- Packed bed
In
chemical process ing, a packed bed is a hollow tube, pipe, or other vessel that is filled with a packing material. The packing can be randomly filled with small objects likeRaschig ring s or else it can be a specifically designedstructured packing .The purpose of a packed bed is typically to improve contact between two phases in a chemical or similar process. Packed beds can be used in a
chemical reactor , adistillation process, or ascrubber , but packed beds have also been used to storeheat in chemical plants. In this case, hot gases are allowed to escape through a vessel that is packed with arefractory material until the packing is hot. Air or other cool gas is then fed back to the plant through the hot bed, thereby pre-heating the air or gas feed.Applications
In industry, a packed column is a type of packed bed used to perform
separation process es, such asabsorption , stripping, anddistillation . A packed column is apressure vessel that has a packed section.cite book|author=Seader, J.D. and Henley, Ernest J.|title=Separation Process Principles|edition=2nd Edition|publisher=John Wiley & Sons|year=2006|id=ISBN 0-471-46480-5] The column can be filled with random dumped packing orstructured packing sections, which are arranged or stacked. In the column, liquids tend to wet the surface of the packing and the vapors pass across this wetted surface, wheremass transfer takes place. Packing material can be used instead of trays to improve separation in distillation columns. Packing offers the advantage of a lower pressure drop across the column (when compared to plates or trays), which is beneficial while operating under vacuum. Differently shaped packing materials have different surface areas and void space between the packing. Both of these factors affect packing performance.Another factor in performance, in addition to the packing shape and surface area, is the liquid and vapor distribution that enters the packed bed. The number of theoretical stages required to make a given separation is calculated using a specific vapor to liquid ratio. If the liquid and vapor are not evenly distributed across the superficial tower area as it enters the packed bed, the liquid to vapor ratio will not be correct and the required separation will not be achieved. The packing will appear to not be working properly. The "height equivalent to a theoretical plate" (HETP) will be greater than expected. The problem is not the packing itself but the mal-distribution of the fluids entering the packed bed. These columns can contain liquid distributors and redistributors which help to distribute the liquid evenly over a section of packing, increasing the efficiency of the mass transfer. The design of the liquid distributors used to introduce the feed and reflux to a packed bed is critical to making the packing perform at maximum efficiency.
Packed columns have a continuous vapor-equilibrium curve, unlike conventional tray distillation in which every tray represents a separate point of vapor-liquid equilibrium. However, when modeling packed columns it is useful to compute a number of theoretical plates to denote the separation efficiency of the packed column with respect to more traditional trays. In design, the number of necessary theoretical equilibrium stages is first determined and then the packing height equivalent to a theoretical equilibrium stage, known as the "height equivalent to a theoretical plate" (HETP), is also determined. The total packing height required is the number theoretical stages multiplied by the HETP.
Columns used in certain types of
chromatography consisting of a tube filled with packing material can also be called packed columns and their structure has similarities to packed beds.Packed bed reactors can be used in chemical reaction. These reactors are tubular and are filled with solid catalyst particles, most often used to catalyze gas reactions. cite book|author=Fogler, H. Scott|title=Elements of Chemical Reaction Engineering|edition=4th Edition|publisher=Prentice Hall|year=2006|id=ISBN 0-13-047394-4] The chemical reaction takes place on the surface of the
catalyst . The advantage of using a packed bed reactor is the higher conversion per weight of catalyst than other catalytic reactors. Thereaction rate is based on the amount of the solid catalyst rather than the volume of the reactor.Theory
The Ergun equation can be used to predict the pressure drop along the length of a packed bed given the fluid
velocity , the packing size, and theviscosity anddensity of the fluid.ee also
*Height of a theoretical plate (HETP)
*Continuous distillation
*Kozeny-Carman equation
*Fluidized bed References
External links
* [http://www.cheresources.com/packcolzz.shtml Packed Column Design]
* [http://www.engin.umich.edu/~cre/asyLearn/bits/pbr/index.htm Packed Bed Reactor Design]
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